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The title compound was prepared from monomethyl sulfate and sodium acetyl ethenoxide, which was obtained from the reaction of acetone, sodium methoxide and methyl formate.The overall yield was 71.8%?
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丙酮、甲醇钠与甲酸甲酯反应得乙酰基乙烯醇钠;再与硫酸氢甲酯反应得到目标产物;收率可达71.;8%25。
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