The state changes of the methylamine molecules in synthesis process of boron-containing CF-2 transformed from porous glass granules were studied using 13C MAS NMR and TG techniques.

• 13C MAS NMR和TG证实模板剂甲胺分子在反应过程中经历了三种状态：在反应初期，甲胺分子与多孔玻璃粉表面羟基处于弱相互作用状态；