The influence of particle size of the starting materials, reaction temperature and holding time are studied experimentally. The phase composition and microstructure of the product are analyzed by means of XRD SEM and EDS.

• 实验研究了原料的初始粒度、反应温度以及保温时间对氮化合成反应的影响,借助XRD、SEM和EDS等分析测试手段测定和观察了产物的物相组成和显微形貌。