The experimental condition of acetylating method for determining priminary alcohol and secondary alcohol catalyzed by perchloric acid in the medium of analytically pure ethylacetate is proposed.

• 提出了以高氯酸为催化剂,分析纯乙酸乙酯为介质,乙酰化法测定伯、仲醇的实验条件,实现了对经典方法的改进,简化了操作程