Methods: Phenol was phosphorylated by DIPPH and DEPH respectively by Atherton Todd reaction,by dropping the DIPPH and DEPH and tetrachloromethane into the mixed solution of phenol,triethylamine and dioxane.

• 方法 :冰盐浴条件 ,DIPPH(DEPH)和四氯化碳的混合液逐滴加到苯酚 ,三乙胺 ,二氧六环的混合液中。