Five N-3-phenyl-acryloyl amino-acids were synthesized through interaction between 3-phenyl-acryloyl chloride and amino-acids in acetone-water in 50%~85% yield .

• 以3-苯基丙烯酸为原料；经酰氯化得3-苯基丙烯酰氯；以丙酮和水混合溶剂为反应介质；和氨基酸反应制得5种未见文献报道的氨基酸N-酰化衍生物；收率在50%25~85%25.