2-iodoethyl methyl ether was synthesized from ethylene glycol monomethylether by chlorination with thionyl chloride and halogen exchange with sodium iodide in total yield 78.9%.

• 以乙二醇单甲醚为原料；经氯化亚砜氯代和碘化钾卤素交换反应得到了2-碘乙基甲基醚；总收率78.；9%25。